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Re: Background to our discussion
- To: Chemical information in core CIF <corecifchem@iucr.org>
- Subject: Re: Background to our discussion
- From: Howard Flack <Howard.Flack@cryst.unige.ch>
- Date: Tue, 11 Nov 2003 18:01:57 +0100
- Organization: University of Geneva
- References: <Pine.SOL.4.33.0310151554490.26288-100000@mcmail.cis.mcmaster.ca>
> Please send any comments to the 'reply to' address before > November 15. Might even make it on time for once. > 2. Background I wish to caution that there are problems with reducing the description of a crystal pattern to that of a set of points. The symmetry of a set of points is not the same as the symmetry of a set of atoms occupying those points. e.g. take the sodium chloride structure and replace each atom by a point. NaCl structure occurs in a cubic F space group, whereas the related structure with atoms replaced by points is primitive. Likewise David talks about a point which is the centre of mass of the molecule. You can not find this just from the coordinates of the points representing the centre of mass of each atom - you need the mass as well. In my mind a crystal structure looks more naturally like a set of atoms (each with a position given by the coordinates of its centre of mass and other properties like element type) rather than a set of points (of known coordinates which acquire elemental properties). > to consider how to identify molecules and other chemical entities Before finding a way to identify these entities we need to be sure we agree on what we consider to be a molecule or 'other chemical entities'. I feel that it is not our problem to define these. We should use definitions acceptable and accepted by chemists. I hope that IUPAC has something to meet these needs. This is critical for the description of molecular symmetry. E.g. if polyethylene is not a molecule, we can stick with point groups to describe the symmetry properties of molecules; if polyethylene is a molecule, I recommend you all go out and immediately buy a copy of International Tables for Crystallography Volume E. > Atoms, .... are ... chemical rather than crystallographic entities. You have already seen that I don't quite agree. > 4. Chemical entities and properties we may wish to define: Of course you all know that chemically-equivalent molecules may not be crystallography-equivalent. However we have to face up to the horrid truth that crystallography-equivalent molecules may not be chemically-equivalent! > 4.1.1 Atoms: Add name (label) and chirality. > 4.1.3 Molecules: Add name, quadruple moment. The optical rotation is a property of the compound or substance not of the molecule. I also have a fancy that sets or collections of molecules need a name. In all of this, racemates are going to be a nightmare. > In all the above cases the atoms used in defining the chemical > properties must be linked to the crystallographic positions they > occupy. The current 'ORTEP'-like code for doing translations in symmetry-related atoms needs a rethink. -5 to +4 is not enough. If the molecule is allowed to have translational symmetry, some other technique is necessary. > 5.4 > It is the only item in the > chemical category that is not related to the crystal. I'm not quite sure what you are driving at in this sentence. In my view something like 'chemical_absolute_configuration' is definitely only related to a particular molecule and has nothing to do at all with the crystal, whereas '_chemical_optical_rotation' is a property of the whole substance (of the crystals taken into solution) and is not the property of an individual molecule. H. _______________________________________________ coreCIFchem mailing list coreCIFchem@iucr.org http://scripts.iucr.org/mailman/listinfo/corecifchem
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